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Testing dissolved non-volatile matter (NVM) or non-volatile residue (NVR) involves evaporating a liquid sample's solvent under controlled heating (often
105∘
𝐶
) to leave behind solid, non-evaporating residues. This gravimetric analysis precisely measures polymers, pigments, or fillers in coatings, inks, and lubricants. 
Key Aspects of NVM/NVR Testing: 
  • Methodology: A sample is weighed, heated in a dish (often to
    105∘
    𝐶
    per ASTM D1353) until the solvent evaporates, and the remaining residue is cooled in a desiccator and weighed.
  • Common Applications: Widely used for paints, coatings, resins, adhesives, and pharmaceutical ingredients to ensure product consistency.
  • Precision: High-precision electronic balances are required (repeatability up to
    0.05
    mg
    ) to accurately measure small amounts of residue, according to Labthink and this YouTube video.
  • Key Standards: Common methods include ASTM D1353 (solvents), ASTM D2369 (coatings), and ISO 3251 (polymers).
  • Solvent Selection: Acetone is often preferred for residue removal in solvent tests, say Scribd. 
Procedure Overview: 
  1. Preparation: Weigh an empty, clean container (tare).
  2. Sampling: Place a specific amount of the material into the container.
  3. Heating: Evaporate the solvent in an oven at a set temperature (e.g.,
    105∘
    𝐶
    ).
  4. Cooling & Final Weighing: Cool the sample in a desiccator, then weigh the residue.
  5. Calculation:
    Weight of residueWeight of sample
    ×100
    %
    =
    %
    NVM
    .
     
Note: For aqueous systems or emulsions, use caution to avoid skinning or splashing. 
  • Determination of nonvolatile matter and the calculation of 'cut ...
    container usually states the cut of the shellac varnish; for example, "4 pounds per gallon" or "4-pound cut." This statement does ...
    National Institute of Standards and Technology (.gov)
  • Non-Volatile Residue (NVR) Testing System - Labthink
    Non-Volatile Residue (NVR)Testing System & Solutions Non-volatile residue (NVR) testing is performed by gravimetric analysis using...
    en.labthink.com
  • Non volatile matter ISO 3251 [Paint Testing]
    Mar 25, 2021 — Non volatile matter ISO 3251 [Paint Testing] - YouTube. 1x. This content isn't available. ISO 3251 test method - table A.2 method ...
    1:16
    YouTube·Spektrochem Paint Technical Center
  • Non-Volatile Matter NVM Industrial Applications Guide - Infinita Lab
    Apr 9, 2026 — Precise NVM analysis ensures material consistency in industrial batches. * Non-Volatile Matter (NVM) Testing is a laboratory test ...
    Infinita Lab
  • Non-Volatile Matter (NVM) Analysis Guide | ASTM D2369 ...
    Apr 8, 2026 — Adhesive NVM is determined by spreading a defined mass on glass or aluminium foil and heating at 105°C for a defined time. For pre...
    Infinita Lab
  • Non-Volatile Residue Test – Gravimetric Determination of ...
    Mar 7, 2018 — clean has different meanings in different contexts whilst dirt can be invisible to the human eye even the smallest amount of conta...
    2m
    YouTube·Laboratory Solutions from METTLER TOLEDO
  • ASTM D1353 Volatile Solvent Nonvolatile Matter Testing - Infinita Lab
    Overview. ASTM D1353 is a widely used test method for determining the percentage of nonvolatile matter present in materials that a...
    Infinita Lab
  • How is non-volatile-matter content determined? - NBchao.Com
    It is recommended that the dish should be covered during the weighing process. For volatile samples, it is recommended to put the ...
    南北潮商城
  • Non-Volatile Matter Test Procedure | PDF - Scribd
    To test for non-volatile matter (NVM), a portion of the sample is placed in a petri dish and heated to evaporate the acetone, leav...
    Scribd
  • Determination of nonvolatile matter and the calculation of 'cut ...
    container usually states the cut of the shellac varnish; for example, "4 pounds per gallon" or "4-pound cut." This statement does ...
    National Institute of Standards and Technology (.gov)
  • Non-Volatile Residue (NVR) Testing System - Labthink
    Non-Volatile Residue (NVR)Testing System & Solutions Non-volatile residue (NVR) testing is performed by gravimetric analysis using...
    en.labthink.com
  • Non volatile matter ISO 3251 [Paint Testing]
    Mar 25, 2021 — Non volatile matter ISO 3251 [Paint Testing] - YouTube. 1x. This content isn't available. ISO 3251 test method - table A.2 method ...
    1:16
    YouTube·Spektrochem Paint Technical Center
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Videos
Non volatile matter ISO 3251 [Paint Testing]
YouTube · Spektrochem Paint Technical Center
Mar 25, 2021
YouTube · Spektrochem Paint Technical Center
1:16
Non-Volatile Residue Test – Gravimetric Determination of ...
YouTube · Laboratory Solutions from METTLER TOLEDO
Mar 7, 2018
YouTube · Laboratory Solutions from METTLER TOLEDO
3:07
Verify cleanliness by analyzing nonvolatile residue (NVR). Rinse with solvent, evaporate, and weigh residue with a microbalance.
Determination of non volatile content
YouTube · EAGLE CHEMICALS
Dec 4, 2019
YouTube · EAGLE CHEMICALS
2:19
8 key moments8 key moments in this video

View all

Web results

Determination of nonvolatile matter and the calculation of ' ...


National Institute of Standards and Technology (.gov)
https://nvlpubs.nist.gov › nistpubs › jres
National Institute of Standards and Technology (.gov)
https://nvlpubs.nist.gov › nistpubs › jres
PDF
It was the purpose of the tests reported in this paper to ascertain how well the amounts of shellac found in varnishes by each of the three methods agree with.Read more
8 pages

How Nonvolatile Residue Detection Works


The Precision Companies
https://www.precgroup.com › PFC
The Precision Companies
https://www.precgroup.com › PFC
The principle is straightforward: rinse or flush the component's surfaces with a validation test fluid that dissolves and suspends the invisible contamination.Read more

Non-Volatile Matter (NVM) Analysis Guide | ASTM D2369 & ...


Infinita Lab
https://infinitalab.com › Material Testing Service
Infinita Lab
https://infinitalab.com › Material Testing Service
Apr 8, 2026 — NVM directly measures the concentration of film-forming polymers, pigments, fillers, and non-volatile additives in a coating or adhesive.Read more
Missing: dissolved ‎| Show results with: dissolved

Determination of percentage volume of non-volatile matter ...


ISO - International Organization for Standardization
https://www.iso.org › obp
ISO - International Organization for Standardization
https://www.iso.org › obp
This document specifies a method for determining the non-volatile matter by volume (NVV) of coating materials and related products by measuring the density of a ...Read more
Missing: dissolved ‎| Show results with: dissolved

Comprehensive Non-Volatile Testing and Volatile Analysis


Sensory Service Center
https://sensory.ncsu.edu › Flavor Services (OLD)
Sensory Service Center
https://sensory.ncsu.edu › Flavor Services (OLD)
Non-volatile analysis tests quality markers in food that are non-aroma sensory components – things such as organic acids and sugars, protein or fat levels.Read more
Missing: dissolved ‎| Show results with: dissolved

Nonvolatile Residue on Surfaces - DTIC


dtic.mil
https://apps.dtic.mil › sti › pdf › ADA213324
dtic.mil
https://apps.dtic.mil › sti › pdf › ADA213324
PDF
by EN Borson · 1989 · Cited by 4 — ASTM E595-84, "Standard Test Method for Total Mass Loss and Collected. Volatile Condensable Materials from Outgassing in a Vacuum. Environment," ...Read more
49 pages

Innovation And Application Of Non-volatile Detection ...


GBPI
https://www.gbpitester.com › innovation-and-applicatio...
GBPI
https://www.gbpitester.com › innovation-and-applicatio...
Nov 18, 2022 — The non-volatile matter test principle of purified water is to detect the mass of non-volatile matter solids obtained after 100mL of purified ...Read more
Missing: dissolved ‎| Show results with: dissolved

non-volatile residues (NVRs)


Mettler-Toledo
https://www.mt.com › home › Laboratory_weighing
Mettler-Toledo
https://www.mt.com › home › Laboratory_weighing
Missing: dissolved ‎materials

General Test Procedure Non Volatile Matter and Residue ...


Pharma Dekho -
https://pharmadekho.com › general-test-procedure-non-...
Pharma Dekho -
https://pharmadekho.com › general-test-procedure-non-...
Jun 9, 2024 — Place clean and dry evaporating dish in an oven at 105°C for 30 minutes. · Transfer 50 ml accurately measured sample being examined into dish.Read more
Missing: dissolved ‎| Show results with: dissolved
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