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Glass reactors for solid-phase reactions, such as peptide synthesis or solid-liquid catalyst processes, are
specialized borosilicate glass vessels designed for efficient mixing, filtration, and washing within a single unit. These reactors feature jacketed walls for temperature control, PTFE filter plates for separating solids, and bottom discharge valves for easy product recovery, ranging from laboratory to pilot scale.Key Features and Benefits
- Integrated Filtration: Equipped with a bottom PTFE filter plate, allowing users to synthesize, wash, and dry solids without transferring the material.
- High Visibility: Borosilicate glass (GG-17) allows real-time visual monitoring of reactions and solid behavior.
- Temperature Control: Double-layer (jacketed) or triple-layer designs allow for efficient heating or cooling using circulating thermal fluid.
- Superior Mixing: Stirring systems designed for solid suspension ensure high conversion rates.
- Chemical Resistance: Excellent resistance to most chemical agents (except concentrated alkalis and hydrofluoric acid).
Common Applications
- Solid-Phase Peptide Synthesis (SPPS): Automated or manual assembly of peptide chains.
- Solid-Liquid Synthesis: Catalytic reactions requiring separation of catalyst from product.
- Crystallization and Separation: Pharmaceutical and chemical development.
Standard Components
- Jacketed glass vessel
- Stirrer (overhead motor with shaft)
- Filter assembly (typically PTFE/ceramic)
- Vacuum/drainage valve
- Condenser and feed ports
These reactors are available as benchtop units (up to 10L) and large pilot-scale systems, often supported by heavy-duty stainless steel frames, as shown in the YouTube video about the Reactor-Ready Duo jacketed glass reactor.
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